@article{oai:nagoya.repo.nii.ac.jp:00011682, author = {南, 雅代 and Minami, Masayo and 中村, 俊夫 and Nakamura, Toshio}, journal = {名古屋大学加速器質量分析計業績報告書}, month = {Mar}, note = {To investigate the best HCl concentration used for decalcification of a fossil bone without loss of bone organic fractions, various concentrations of 0.4M, 0.6M, 0.8M, 1.0M and 1.2M HCl were examined to analyze carbon, nitrogen and radiocarbon isotopes. The bone used in the experiment is a fossil fragment collected from the Awazu submarine archeological site, Shiga. The yield of insoluble decalcified fractions does not change in the range from 0.4M to 1.0M HCl, and it decreases on 1.2M HCl. The result suggests that a part of bone organic fractions departs from the decalcified fractions by treatment of higher HCl concentration. The ^<14>C age for gelatin collagens does not change on any concentrations of 0.4M, 0.6M, 0.8M and 1.2M HCl, and could be reliable because the XAD-2 treated hydrolysate fraction shows the same ^<14>C age. Therefore, 0.4M is the best concentration of HCl to efficiently decalcify the fossil fragment in this study. The fossil bone used in this study is well-preserved, and the above best condition of decalcification does not apply to another poorly-preserved fossil bones. It could be, however, suitable to decalcify and fossil bone with 0.4M HCl in a cellulose tube., タンデトロン加速器質量分析計業績報告 Summaries of Researches Using AMS 2001 (平成13)年度}, pages = {177--185}, title = {化石骨の脱灰処理条件の検討}, volume = {13}, year = {2002} }