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Gas Chromatographic Analysis of Steroid Hormones Part I. Problems in Quantitative Aspects of Gas Chromatography
https://doi.org/10.18999/nagjms.29.3.191
https://doi.org/10.18999/nagjms.29.3.1915d511231-0e09-4b62-a4c4-69107aff5f3a
名前 / ファイル | ライセンス | アクション |
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v29n3p191_230.pdf (6.4 MB)
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Item type | 紀要論文 / Departmental Bulletin Paper(1) | |||||
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公開日 | 2016-09-27 | |||||
タイトル | ||||||
タイトル | Gas Chromatographic Analysis of Steroid Hormones Part I. Problems in Quantitative Aspects of Gas Chromatography | |||||
言語 | en | |||||
著者 |
YASUDA, KANAE
× YASUDA, KANAE |
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アクセス権 | ||||||
アクセス権 | open access | |||||
アクセス権URI | http://purl.org/coar/access_right/c_abf2 | |||||
抄録 | ||||||
内容記述タイプ | Abstract | |||||
内容記述 | In an attempt to evaluate gas chromatography for quantitative use, relative peak area ratio (RPAR) was studied under various analytical conditions and several problems in the quantitative analysis were elucidated. The loss was influenced by the sample size, structure of the steroid, retention time, operating temperature, loading effect and gas chromatographic appartaus. Problems relating to matters of instrumental design and column packing inclusive were of the most importance. In certain instances trimethylsilyl ethers were useful for avoiding these difficulties but these derivatives and even saturated hydrocarbons were not found to be recovered completely in gas chromatography. Of the various causes proposed for this phenomenon, adsorption appeared to be the most siginificant. When precise estimation is required, it should not be extended beyond a certain limit even by employing suitable operating conditions. Relatively reliable procedures for careful control of routine estimation are outlined. As a matter of course, the necessity for proper instrumentation should also be emphasized and the properties of any given equipment, analytical conditions and the accuracy of the obtained data should be checked with the RPAR curve. | |||||
言語 | en | |||||
出版者 | ||||||
出版者 | Nagoya University School of Medicine | |||||
言語 | en | |||||
言語 | ||||||
言語 | eng | |||||
資源タイプ | ||||||
資源タイプ識別子 | http://purl.org/coar/resource_type/c_6501 | |||||
資源タイプ | departmental bulletin paper | |||||
出版タイプ | ||||||
出版タイプ | VoR | |||||
出版タイプResource | http://purl.org/coar/version/c_970fb48d4fbd8a85 | |||||
ID登録 | ||||||
ID登録 | 10.18999/nagjms.29.3.191 | |||||
ID登録タイプ | JaLC | |||||
関連情報 | ||||||
関連タイプ | isVersionOf | |||||
識別子タイプ | URI | |||||
関連識別子 | http://www.med.nagoya-u.ac.jp/medlib/nagoya_j_med_sci/293/293.html | |||||
ISSN(print) | ||||||
収録物識別子タイプ | PISSN | |||||
収録物識別子 | 0027-7622 | |||||
ISSN(Online) | ||||||
収録物識別子タイプ | EISSN | |||||
収録物識別子 | 2186-3326 | |||||
書誌情報 |
en : Nagoya Journal of Medical Science 巻 29, 号 3, p. 191-230, 発行日 1967-01 |
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著者版フラグ | ||||||
値 | publisher |