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  1. I500 未来社会創造機構
  2. I500a 雑誌掲載論文
  3. 学術雑誌

Multiple phase separation of super-abundant-vacancies in Pd hydrides by all solid-state electrolysis in moderate temperatures around 300 °C

http://hdl.handle.net/2237/25240
http://hdl.handle.net/2237/25240
e5d9974f-39a8-4cfd-aee4-c352f512d44b
名前 / ファイル ライセンス アクション
sav2_paper_riv_submit.pdf sav2_paper_riv_submit.pdf ファイル公開:2018/12/01 (2.7 MB)
Item type 学術雑誌論文 / Journal Article(1)
公開日 2016-12-16
タイトル
タイトル Multiple phase separation of super-abundant-vacancies in Pd hydrides by all solid-state electrolysis in moderate temperatures around 300 °C
言語 en
著者 Fukada, Yoshiki

× Fukada, Yoshiki

WEKO 68182

en Fukada, Yoshiki

Search repository
Hioki, Tatsumi

× Hioki, Tatsumi

WEKO 68183

en Hioki, Tatsumi

Search repository
Motohiro, Tomoyoshi

× Motohiro, Tomoyoshi

WEKO 68184

en Motohiro, Tomoyoshi

Search repository
アクセス権
アクセス権 open access
アクセス権URI http://purl.org/coar/access_right/c_abf2
権利
言語 en
権利情報 © 2016. This manuscript version is made available under the CC-BY-NC-ND 4.0 license http://creativecommons.org/licenses/by-nc-nd/4.0/
抄録
内容記述 The dynamics of hydrogen-induced vacancies are the key for understanding various phenomena in metal–hydrogen systems under a high hydrogen chemical potential. In this study, a novel dry-electrolysis experiment was performed in which a hydrogen isotope was injected into a Pd cathode and time-resolved in situ monochromatic X-ray diffraction measurement was carried out at the Pd cathode. It was found that palladium-hydride containing vacancies forms multiple phases depending on the hydrogen chemical potential. Phase separation into vacancy-rich, vacancy-poor, and moderate-vacancy-concentration phases was observed when the input voltage was relatively low, i.e., ∼0.5 V. The moderate-vacancy-concentration phase may be attributed to Ca7Ge or another type of super-lattice Pd7VacH(D)8. Transition from the vacancy-rich to the moderate-vacancy-concentration phase explains the sub-micron void formations without high temperature treatment that were observed at the Pd cathode but have never been reported in previous anvil experiments.
言語 en
内容記述タイプ Abstract
出版者
言語 en
出版者 Elsevier
言語
言語 eng
資源タイプ
資源タイプresource http://purl.org/coar/resource_type/c_6501
タイプ journal article
出版タイプ
出版タイプ AM
出版タイプResource http://purl.org/coar/version/c_ab4af688f83e57aa
DOI
関連タイプ isVersionOf
識別子タイプ DOI
関連識別子 https://doi.org/10.1016/j.jallcom.2016.07.176
ISSN
収録物識別子タイプ PISSN
収録物識別子 0925-8388
書誌情報 en : Journal of Alloys and Compounds

巻 688B, p. 404-412, 発行日 2016-12
著者版フラグ
値 author
URI
識別子 http://dx.doi.org/10.1016/j.jallcom.2016.07.176
識別子タイプ DOI
URI
識別子 http://hdl.handle.net/2237/25240
識別子タイプ HDL
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