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Preparation of zinc oxide with a three-dimensionally interconnected macroporous structure via a sol–gel method accompanied by phase separation
http://hdl.handle.net/2237/00030880
http://hdl.handle.net/2237/00030880b9bdfcda-349d-4d56-848f-de2c3dda29b3
名前 / ファイル | ライセンス | アクション |
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Item type | 学術雑誌論文 / Journal Article(1) | |||||
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公開日 | 2019-11-14 | |||||
タイトル | ||||||
タイトル | Preparation of zinc oxide with a three-dimensionally interconnected macroporous structure via a sol–gel method accompanied by phase separation | |||||
言語 | en | |||||
著者 |
Lu, Xuanming
× Lu, Xuanming× Kanamori, Kazuyoshi× Nakanishi, Kazuki |
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アクセス権 | ||||||
アクセス権 | open access | |||||
アクセス権URI | http://purl.org/coar/access_right/c_abf2 | |||||
抄録 | ||||||
内容記述 | A facile method for the preparation of zinc oxide with three-dimensionally (3D) interconnected macropores has been developed. The Zn-based monolithic gel was obtained using citric acid (CA) as a structure supporter via an epoxide-mediated sol–gel method accompanied by phase separation. The size of the macropores could be controlled by the ratio of methanol to propylene oxide in the starting solution. The Zn-based gel was heat-treated in air with the purpose of removing the organic components and crystallizing the ZnO, finally resulting in pure ZnO (purity >90%, with negligible carbon content) with 3D interconnected macropores and an open nanoscale network. The influence of the starting solvent composition on the Zn-based gel morphologies has been examined and discussed based on the chemical compatibility of the Zn–CA complex with other components. | |||||
言語 | en | |||||
内容記述タイプ | Abstract | |||||
内容記述 | ||||||
内容記述 | ファイル公開:2020/08/07 | |||||
言語 | ja | |||||
内容記述タイプ | Other | |||||
出版者 | ||||||
言語 | en | |||||
出版者 | Royal Society of Chemistry | |||||
言語 | ||||||
言語 | eng | |||||
資源タイプ | ||||||
資源タイプresource | http://purl.org/coar/resource_type/c_6501 | |||||
タイプ | journal article | |||||
出版タイプ | ||||||
出版タイプ | AM | |||||
出版タイプResource | http://purl.org/coar/version/c_ab4af688f83e57aa | |||||
DOI | ||||||
関連タイプ | isVersionOf | |||||
識別子タイプ | DOI | |||||
関連識別子 | https://doi.org/10.1039/C9NJ02373A | |||||
ISSN(print) | ||||||
収録物識別子タイプ | PISSN | |||||
収録物識別子 | 1144-0546 | |||||
書誌情報 |
en : New Journal of Chemistry 巻 43, 号 29, p. 11720-11726, 発行日 2019-08-07 |
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著者版フラグ | ||||||
値 | author |